==== SHADOWS Micro Spectro-Gonio Radiometer ==== ---- === Laboratory Experiment facility === **Facility name:** Micro Spectro-Gonio Radiometer **Location:** Institut de Planétologie et Astrophysique de Grenoble (IPAG) CNRS - Université Grenoble Alpes Saint Martin d’Hères, France **Persons in charge:** - Scientific : Pierre Beck, Assistant Professor & Bernard Schmitt, Research director - Technical : Olivier Brissaud, Engineer ---- **General description** The new micro spectro-gonio radiometer currently under developement will be optimized for the measurement at low temperature of bidirectional reflectance spectra, over the visible and near-IR (at least from 350 to 4800 nm), of dark and very small samples (organics, meteorites…) down to a few mm3 in volume. [[sample holders]]: It will have 2 major sample holder configurations: - //Open sample holders// (various sizes) in //cold chamber// over -20°C ─ +20°C temperature range. - The //SERAC environmental// cell with cryostats, pumps, pressure and temperature controllers, which allows us to introduce gas(es) of known composition and pressure (10-6 mb - 1 bar) over the sample and controlling and measuring the temperature over the -40°C ─ +80°C range. It will have a set of sample holders (small sizes) adapted to this new setup. [[Tools and sub-systems]]: A number of sample preparation tools and experiment sub-systems are available to the facility: - For samples preparation: another cold chamber (down to -20°C), set of sample holders, several specific tools for ice sample preparation, 2 sets of sieves, grinders, mortars, saw, balances, microscope, owen, ultra-pure water, several pure gasses, wet chemistry materials a, several owens (up to 1200°C) for sample treatments. - For the experiment: a thermodynamic volumetric system with high accuracy pressure gauges (10-6 to 1 bar), a flow meter (1-10 sccm) and pumps. He-Ne laser + detectors, camera for sample monitoring, … ---- **Technical characteristics:** [[Spectral range]] : 0.35 - 4.5 µm (< 0.35 & > 4.8 µm: lower S/N) (4.2-4.3µm: atm. CO2 limited) [[Spectral resolution]] : variable - mini: < 0.1 nm (but S/N limited) - maxi: 3 nm (<700nm), 7 nm (<1600nm), 12 nm (<3000nm), 26nm (>3000nm) [May change with future new monochromator] [[Bidirectional Reflectance]] - ''Incidence angle'': 0° to 75° ; resolution: 2° (can be reduced to 1°) ; maximum sampling : 0.1° - ''Emergence angle'': 0° to 80° for dark / fine grained samples ; resolution : ± 2° (may be reduced to < ± 0.5°, but S/N limited) ; max. sampling : 0.1° - ''Azimuth angle'': 0° to 180° ; resolution : ± 2° (may be reduced to < ± 0.5°, but S/N limited) ; max. sampling : 0.1° - ''Phase angle'': up to to 155° ; mini : ~ 7° for dark / fine grained samples - ''Illumination diameter'' (nadir): 7.5 mm - ''Observation diameter'' (nadir): 20 mm [[Photometry]]: ''Absolute'': [will be determined during calibration and test phase end 2015 - 2016] - 0.35-1.0 µm: expected better than 1% over all configurations (relative to a calibrated Spectralon 0.99 reference panel) - 1.0-2.5 µm: expected better than 1% over all configurations - 2.5-4.5 µm : expected better than 2% over all configurations ''Relative'' : - better than 0.5% (0.35-4.5 µm) [[File:micro-gonio_design-optique.jpg|500px]] ''Picture'': sketch of the micro spectro-gonio radiometer under building at IPAG [[Samples]] ''Types'': cosmo-materials, synthetic and terrestrial carbonaceous materials, minerals ''Texture'': compact (dark) or granular (dark and/or fine grained < 200µm) ''Grain size'': sub-µm to a 200 µm ''Size'': - 32 mm diameter (for full BRDF down to 75° observation) - 8 mm x 32 mm (for principal plane observation down to 75°) - 8 mm x 16 mm (for principal plane observation down to 60°) ''Thickness'': - 0.1 mm for dark & fine grained samples (< 20 µm) - up to 5 mm for 'gray' & medium grained samples (< 200 µm) - up to 10 mm for bright & medium/fine grained samples (< 100 µm) [[Temperature]]: - room temperature or heated - down to -20°C (in cold room) - down to -40°C (in SERAC environmental cell) [[Experiment control]]: - PC/Windows, fully software controlled (LabView©). Automatic acquisition of all spectral/geometric configurations [[Acquisition time]]: [will be determined during calibration and test phase end 2015 - 2016] - typical: 1 mn for 200 spectral channels in visible (S/N dependent) - total: <1 hour for 100 spectral channels and 100 geometries [[Current state of system]]: - Visible 0.3 - 1 µm range: under development, testing and buiding [2013-2015]. Ready for full testing end of 2015 - Infrared 1 - 4.8µm range: extension planned in 2015-2017 (if EPN2020-RI program accepted) - low temperature: to be tested in cold room down to -20°C (end 2015) * Characteristics: Micro-Spectro-Gonio_characteristics.pdf **(TBD)** * Article: **Availability to community:** //**2016-2017:**// - Technical improvements/calibration (40%) - IPAG + associated laboratories measurements (60%) //**after 2017:**// - Technical improvements/calibration (20%) - IPAG + associated laboratories measurements (60%) - open as facility or to specific collaborations w. funding (20%) ---- **References:**